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Beilstein J. Nanotechnol. 2016, 7, 995–1009, doi:10.3762/bjnano.7.92
Scheme 1: Synthesis of complexes 1–3. (a) NaH, 1/3DyCl3·6H2O, EtOH, reflux then stirring at RT overnight. (b)...
Scheme 2: Synthesis of complex 4 under anhydrous conditions. The proposed structure of the complex is based o...
Figure 1: Molecular structure of complex 1 obtained by single crystal X-ray diffraction. Hydrogen atoms are o...
Figure 2: Molecular structure of complex 2 obtained by single crystal X-ray diffraction. Hydrogen atoms are o...
Figure 3: Molecular structure of complex 3 obtained by single crystal X-ray diffraction. Hydrogen atoms are o...
Figure 4: Absorption spectra of the three dysprosium complexes in diluted (2 × 10−6 M) DMSO solutions of 1–4 ...
Figure 5: (Top) Temperature dependence of out-of-phase component of ac magnetic susceptibility under zero dc ...
Figure 6: Orientation of the main anisotropy axis in complexes 1–3 indicated as blue arrows (a, b and c) calc...
Figure 7: Cole–Cole plots under zero or different dc fields in the given temperature ranges. Sample codes are...
Beilstein J. Nanotechnol. 2016, 7, 126–137, doi:10.3762/bjnano.7.15
Figure 1: Molecular structure of complex 3 obtained from single-crystal diffraction. Dy(III) ions are marked ...
Figure 2: (a) Experimental χMT(T) and fitting (red trace) for compound 1 (parameters for fitting are describe...
Figure 3: Molar magnetic susceptibility (χMT) vs T plot for 2–5 under 0.1 T DC field and molar magnetization (...
Figure 4: Experimental dynamic magnetic behavior for 3. (a) χ"M(T) measured under a zero field (3.5 Oe AC fie...
Figure 5: Experimental dynamic magnetic behavior for 5. (a) χ"M(T) measured under an applied DC field of 800 ...
Figure 6: Single-crystal measurements of M(H)/MS vs µ0H measured on a micro-SQUID array for 3 (a) at 0.03 K a...
Figure 7: Magnetic axes obtained through the electrostatic method: (a) side and (b) top view for compound 3. ...
Figure 8: STM topography of 2 after deposition on Au(111). Image sizes are (a) 60 × 60 nm2 and (c) 20 × 20 nm2...
Beilstein J. Nanotechnol. 2013, 4, 807–814, doi:10.3762/bjnano.4.92
Figure 1: Molecular structure of [Fe4Dy2(OH)2(N-nbdea)4((CH3)3CCOO)6(N3)2] and its core. Solvent molecules, d...
Figure 2: The 57Fe Mössbauer spectra for [Fe4Dy2(OH)2(N-nbdea)4((CH3)3CCOO)6(N3)2] at 100 and 50 K (top); at ...
Figure 3: χT-vs-T plots at 0.1 T for 1 and 2 (inset). The solid line is the best fit to the experimental data....
Figure 4: 3 K Mössbauer spectrum of polycrystalline 2 recorded in a perpendicularly applied field of 5.0 T. T...
Figure 5: Plot of out-of-phase ac susceptibility signals vs temperature for 1 at the indicated oscillation fr...